7F36
TacT complexed with acetyl-glycyl-tRNAGly
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-1A |
Synchrotron site | Photon Factory |
Beamline | BL-1A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-12-02 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 1.00 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 52.743, 121.873, 127.257 |
Unit cell angles | 90.00, 91.07, 90.00 |
Refinement procedure
Resolution | 49.040 - 3.098 |
R-factor | 0.2112 |
Rwork | 0.208 |
R-free | 0.26310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5fvj |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.040 | 3.210 |
High resolution limit [Å] | 3.098 | 3.100 |
Rmerge | 0.237 | 1.411 |
Number of reflections | 29107 | 2823 |
<I/σ(I)> | 7.6 | 1.3 |
Completeness [%] | 99.3 | |
Redundancy | 7.1 | |
CC(1/2) | 0.994 | 0.606 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 200mM calcium acetate, 100mM sodium cacodylate, pH 6.0, 14% (v/v) PEG 8000 |