7F2W

TbUox in complex with uric acid

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSRRC BEAMLINE BL13B1
Synchrotron site	NSRRC
Beamline	BL13B1
Temperature [K]	100
Detector technology	CCD
Collection date	2019-03-19
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.00000
Spacegroup name	I 4 2 2
Unit cell lengths	146.362, 146.362, 132.407
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.580 - 2.160
R-factor	0.1598
Rwork	0.158
R-free	0.19890
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6oe8
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX (1.17.1_3660)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	28.580	2.230
High resolution limit [Å]	2.160	2.160
Number of reflections	38278	3502
<I/σ(I)>	92.3
Completeness [%]	99.8
Redundancy	6.7
CC(1/2)	0.970	0.907

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		283	sodium cacodylate trihydrate, magnesium acetate tetrahydrate, PEG8000