7EYM
Crystal structure of Vibrio cholerae ppnP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-05-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97915 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 55.242, 55.242, 111.851 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.380 |
R-factor | 0.2064 |
Rwork | 0.205 |
R-free | 0.22480 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7eyj |
RMSD bond length | 0.007 |
RMSD bond angle | 0.858 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | REFMAC (v1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.430 |
High resolution limit [Å] | 1.380 | 1.380 |
Rmerge | 0.112 | 0.901 |
Rmeas | 0.117 | 0.976 |
Rpim | 0.032 | 0.364 |
Number of reflections | 35454 | 6596 |
<I/σ(I)> | 26.333 | 1.667 |
Completeness [%] | 99.6 | 97.1 |
Redundancy | 12.5 | 6.4 |
CC(1/2) | 0.994 | 0.576 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M Ammonium sulfate, 30% w/v Polyethylene glycol 8,000 |