7ETL
The crystal structure of FtmOx1-Y68F
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-12 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97853 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 60.252, 45.383, 104.963 |
Unit cell angles | 90.00, 100.26, 90.00 |
Refinement procedure
Resolution | 27.705 - 1.992 |
R-factor | 0.173886221329 |
Rwork | 0.171 |
R-free | 0.22024 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ZON |
RMSD bond length | 0.007 |
RMSD bond angle | 0.862 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | HKL-3000 |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.020 |
High resolution limit [Å] | 1.990 | 1.990 |
Rmerge | 0.175 | 0.877 |
Number of reflections | 38521 | 1881 |
<I/σ(I)> | 10.125 | |
Completeness [%] | 99.9 | |
Redundancy | 6.1 | |
CC(1/2) | 0.989 | 0.539 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M Bis-tris pH 7.0, 1.9 M ammonium sulfate,0,05 M CoCl2 |