7ESV
Structure and mutation analysis of the hexameric P4 from Pseudomonas aeruginosa phage phiYY
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-21 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.979 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 155.630, 67.930, 107.650 |
Unit cell angles | 90.00, 128.94, 90.00 |
Refinement procedure
Resolution | 33.570 - 2.180 |
R-factor | 0.2135 |
Rwork | 0.212 |
R-free | 0.25470 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4blp |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.570 | 2.240 |
High resolution limit [Å] | 2.180 | 2.180 |
Number of reflections | 304717 | 22749 |
<I/σ(I)> | 8 | |
Completeness [%] | 99.3 | |
Redundancy | 6.7 | |
CC(1/2) | 0.993 | 0.640 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.9 | 291 | 200 mM NH4 tartrate, 20% PEG2000 MME, phosphate pH 7.9 |