7EHO

Chitin oligosaccharide binding protein

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL26B1
Synchrotron site	SPring-8
Beamline	BL26B1
Temperature [K]	100
Detector technology	CCD
Collection date	2016-09-28
Detector	RAYONIX MX225HE
Wavelength(s)	1.0
Spacegroup name	P 1 21 1
Unit cell lengths	61.782, 75.978, 87.493
Unit cell angles	90.00, 107.13, 90.00

Refinement procedure

Resolution	41.810 - 1.790
R-factor	0.1795
Rwork	0.178
R-free	0.20700
Structure solution method	SAD
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX (1.18.2_3874)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.830
High resolution limit [Å]	1.790	1.790
Rmeas	0.124	1.313
Rpim	0.048	0.533
Number of reflections	65822	3323
<I/σ(I)>	20.5
Completeness [%]	91.2
Redundancy	6.3
CC(1/2)		0.701

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6	293	PEG3350, MES