7EFS
Fructose-bisphosphate aldolase in Artemisia sieversiana pollen
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ELECTRON MICROSCOPE |
Source details | BRUKER TURBO X-RAY SOURCE |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2020-11-12 |
Detector | AGILENT ATLAS CCD |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 84.007, 129.689, 157.343 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.490 - 2.500 |
R-factor | 0.2119 |
Rwork | 0.209 |
R-free | 0.25850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6rng |
Data reduction software | PHENIX |
Data scaling software | PHENIX |
Phasing software | PHENIX |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 73.930 | 1.570 |
High resolution limit [Å] | 1.550 | 1.550 |
Rmerge | 0.119 | |
Number of reflections | 60088 | 1401 |
<I/σ(I)> | 2.1 | |
Completeness [%] | 79.1 | |
Redundancy | 10.1 | |
CC(1/2) | 0.040 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 5 | 289 | 12%PEG3350,0.1MNaAC |