7EEC
Crystal structure of EphA7 mutant G656R
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2020-11-11 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54184 |
Spacegroup name | P 65 |
Unit cell lengths | 51.780, 51.780, 216.080 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.843 - 3.100 |
Rwork | 0.181 |
R-free | 0.21010 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2rei |
RMSD bond length | 0.008 |
RMSD bond angle | 1.589 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.030 | 3.270 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.175 | 0.175 |
Number of reflections | 5944 | 874 |
<I/σ(I)> | 11.9 | |
Completeness [%] | 100.0 | |
Redundancy | 1 | |
CC(1/2) | 0.984 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295.15 | PEG3350, ammonium sulphate, HEPES |