7E9Y

Crystal structure of eLACCO1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-08-19
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.03
Spacegroup name	C 2 2 21
Unit cell lengths	102.217, 104.983, 138.748
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	52.492 - 2.250
R-factor	0.149
Rwork	0.147
R-free	0.18500
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2zzv 3sg6
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	MOLREP
Refinement software	PHENIX (1.14_3260)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	52.492	2.330
High resolution limit [Å]	2.250	2.250
Number of reflections	35740	3530
<I/σ(I)>	5.75
Completeness [%]	99.9
Redundancy	5.3
CC(1/2)	0.986	0.570

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.2 M Ammonium citrate dibasic 20% w/v PEG 3350