7E34
Crystal structure of SUN1-Speedy A-CDK2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-01-22 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.91905 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 59.340, 183.525, 103.829 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.590 - 3.190 |
R-factor | 0.254 |
Rwork | 0.252 |
R-free | 0.30000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5uq2 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.940 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.310 |
High resolution limit [Å] | 3.190 | 6.890 | 3.200 |
Rmerge | 0.108 | 0.046 | 0.573 |
Rmeas | 0.120 | 0.051 | 0.657 |
Rpim | 0.051 | 0.023 | 0.314 |
Number of reflections | 9795 | 1060 | 928 |
<I/σ(I)> | 5.7 | ||
Completeness [%] | 99.3 | 99.1 | 94.3 |
Redundancy | 5.2 | 5 | 4 |
CC(1/2) | 0.997 | 0.808 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 291 | 0.15M ammonium citrate tribasic, pH7.0, 12% PEG 3350 |