7E2T
Synechocystis GUN4 in complex with phycocyanobilin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-09-29 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 32.465, 64.695, 106.521 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.950 - 1.100 |
R-factor | 0.1267 |
Rwork | 0.125 |
R-free | 0.15630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4xkc |
Data reduction software | HKL-3000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.140 |
High resolution limit [Å] | 1.100 | 1.100 |
Rmerge | 0.148 | 0.820 |
Rpim | 0.050 | 0.270 |
Number of reflections | 91915 | 9050 |
<I/σ(I)> | 15.5 | 2.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 9.6 | 9.7 |
CC(1/2) | 0.994 | 0.838 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | Sodium citrate pH 5.5, PEG 6000 |