7DYM
Pseudomonas aeruginosa TseT-TsiT complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-07-13 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 65 |
Unit cell lengths | 77.500, 77.500, 185.900 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.370 - 3.100 |
R-factor | 0.2079 |
Rwork | 0.206 |
R-free | 0.23720 |
Structure solution method | SAD |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | AutoSol |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.530 | 3.180 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.063 | 0.480 |
Number of reflections | 11293 | 777 |
<I/σ(I)> | 23.34 | |
Completeness [%] | 98.8 | |
Redundancy | 10 | |
CC(1/2) | 0.990 | 0.960 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 0.18 m Trimethylamine N-oxide, 0.1M Tris pH 8.5, 11% PEG2000MME |