7DUU
Crystal structure of HLA molecule with an KIR receptor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 87 |
Detector technology | CCD |
Collection date | 2020-01-05 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 82.056, 153.962, 177.556 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.390 | 2.600 |
High resolution limit [Å] | 2.510 | 2.510 |
Rmerge | 0.083 | 0.561 |
Number of reflections | 38710 | 3797 |
<I/σ(I)> | 11.83 | |
Completeness [%] | 99.0 | |
Redundancy | 6.3 | |
CC(1/2) | 0.961 | 0.867 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 277 | 0.2 M Lithium sulfate, 0.1 M Tris pH 8.5, 25% w/v PEG 3350 |