7DQX
Crystal structure of xanthine dehydrogenase family protein
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2019-12-06 |
Detector | Nonius Kappa CCD |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 112.860, 126.792, 294.490 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 147.240 - 3.440 |
R-factor | 0.2894 |
Rwork | 0.287 |
R-free | 0.32600 |
Structure solution method | SAD |
RMSD bond length | 0.005 |
RMSD bond angle | 1.388 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 147.240 | 3.550 |
High resolution limit [Å] | 3.430 | 3.430 |
Number of reflections | 56814 | 5553 |
<I/σ(I)> | 1.1 | |
Completeness [%] | 96.0 | |
Redundancy | 12.2 | |
CC(1/2) | 0.870 | 0.512 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 4000 |