7DNN
Crystal structure of the AgCarB2-C2 complex with homoorientin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
Synchrotron site | Photon Factory |
Beamline | AR-NE3A |
Temperature [K] | 95 |
Detector technology | PIXEL |
Collection date | 2019-12-06 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 73.905, 102.511, 136.090 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.170 - 2.250 |
R-factor | 0.1989 |
Rwork | 0.196 |
R-free | 0.24710 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 0.935 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | CRANK2 |
Refinement software | PHENIX (1.18_3845) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.970 | 2.370 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmerge | 0.054 | 0.852 |
Number of reflections | 94668 | 13699 |
<I/σ(I)> | 17.49 | |
Completeness [%] | 99.8 | |
Redundancy | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 25%(w/v) PEG4000, 0.1 M MES pH 6.5, 0.2 M Potassium Iodide |