7DN1
Hetero-oligomers of SCR-SCR2 crystal structure with NADPH
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-09-26 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9793 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 69.589, 114.676, 127.752 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.190 - 1.740 |
R-factor | 0.1677 |
Rwork | 0.166 |
R-free | 0.20660 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ctm |
RMSD bond length | 0.012 |
RMSD bond angle | 2.094 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | REFMAC |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.190 | 1.760 |
High resolution limit [Å] | 1.740 | 1.740 |
Number of reflections | 100531 | 3906 |
<I/σ(I)> | 11 | |
Completeness [%] | 98.5 | |
Redundancy | 10.9 | |
CC(1/2) | 0.990 | 0.970 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293.15 | 1 M MES, 30% PEG 300, pH 6.5 |