7DKE
Stenotrophomonas maltophilia DPP7 in complex with Phe-Tyr
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 95 |
Detector technology | PIXEL |
Collection date | 2019-01-27 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 68.035, 74.555, 153.868 |
Unit cell angles | 90.00, 94.44, 90.00 |
Refinement procedure
Resolution | 40.003 - 1.910 |
Rwork | 0.207 |
R-free | 0.25110 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7dkb |
RMSD bond length | 0.010 |
RMSD bond angle | 1.575 |
Data reduction software | xia2 (0.5.764) |
Data scaling software | DIALS (1.12.2) |
Phasing software | REFMAC (5.8.0267) |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.130 | 1.940 |
High resolution limit [Å] | 1.910 | 1.910 |
Rmerge | 0.157 | 1.012 |
Rmeas | 0.170 | |
Rpim | 0.064 | 0.421 |
Number of reflections | 118877 | 5580 |
<I/σ(I)> | 7 | 2 |
Completeness [%] | 99.6 | 93.9 |
Redundancy | 6.9 | 6.7 |
CC(1/2) | 0.991 | 0.631 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 0.2M Ca Acetate, 20%w/v PEG 8000 |