7DJN

Human Serum Albumin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-11-03
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.98
Spacegroup name	P 1
Unit cell lengths	52.092, 53.030, 117.424
Unit cell angles	99.17, 93.45, 117.64

Refinement procedure

Resolution	19.340 - 2.040
R-factor	0.2429
Rwork	0.242
R-free	0.27590
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6m4r
Refinement software	PHENIX (1.17.1_3660)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.520	2.090
High resolution limit [Å]	2.040	2.040
Rmerge	0.076	0.973
Number of reflections	64942	4262
<I/σ(I)>	8.4
Completeness [%]	94.2
Redundancy	1.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	phosphate