7DHW
Crystal structure of myosin-XI motor domain in complex with ADP-ALF4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-20 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.277, 73.725, 187.957 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.810 - 2.840 |
R-factor | 0.2309 |
Rwork | 0.226 |
R-free | 0.27060 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mnd |
RMSD bond length | 0.002 |
RMSD bond angle | 0.490 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 19.810 | 19.810 | 3.010 |
High resolution limit [Å] | 2.840 | 7.900 | 2.840 |
Rmerge | 0.132 | 0.028 | 0.840 |
Rmeas | 0.147 | 0.032 | 0.927 |
Number of reflections | 19625 | 951 | 2992 |
<I/σ(I)> | 11.09 | 40.75 | 2.1 |
Completeness [%] | 99.1 | 92.3 | |
Redundancy | 5.58 | ||
CC(1/2) | 0.997 | 0.999 | 0.855 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 296 | 0.1 M MMT buffer (pH 6.0), 25% PEG-1500 |