7DFU
Crystal structure of Xanthomonas oryzae ClpP S68Y in complex with ADEP4.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-07-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9735 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 132.498, 132.498, 187.833 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.692 - 1.901 |
R-factor | 0.2187 |
Rwork | 0.217 |
R-free | 0.24340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3sta |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (V1.0) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 30.000 | 1.970 |
High resolution limit [Å] | 1.900 | 4.090 | 1.900 |
Rmerge | 0.135 | 0.057 | 0.494 |
Rmeas | 0.140 | 0.059 | 0.556 |
Rpim | 0.032 | 0.012 | 0.243 |
Total number of observations | 2033446 | ||
Number of reflections | 130286 | 13758 | 12105 |
<I/σ(I)> | 5.2 | ||
Completeness [%] | 99.3 | 99.9 | 93.6 |
Redundancy | 15.6 | 22.9 | 4.3 |
CC(1/2) | 0.999 | 0.224 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1 M Sodium acetate trihydrate, 3.0 M Sodium chloride |