7DE7
Crystal structure of PDZD7 HHD domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-04 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97891 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 32.782, 75.005, 42.939 |
Unit cell angles | 90.00, 103.10, 90.00 |
Refinement procedure
Resolution | 37.500 - 1.490 |
R-factor | 0.1784 |
Rwork | 0.177 |
R-free | 0.19360 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6fdd |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 37.500 | 37.500 | 1.580 |
High resolution limit [Å] | 1.490 | 4.460 | 1.490 |
Rmerge | 0.084 | 0.038 | 1.197 |
Rmeas | 0.091 | 0.041 | 1.301 |
Number of reflections | 32592 | 1266 | 5160 |
<I/σ(I)> | 13.49 | 44.52 | 1.56 |
Completeness [%] | 99.4 | 99.6 | 98.2 |
Redundancy | 6.74 | 6.678 | 6.442 |
CC(1/2) | 0.999 | 0.999 | 0.725 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1 M Bis-Tris pH 6.5, 45% Polypropylene glycol P400 |