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7DA0

High-resolution crystal structure of the chicken MHF complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL44XU
Synchrotron siteSPring-8
BeamlineBL44XU
Temperature [K]100
Detector technologyCCD
Collection date2014-04-18
DetectorADSC QUANTUM 210
Wavelength(s)0.9
Spacegroup nameC 1 2 1
Unit cell lengths50.566, 69.071, 48.878
Unit cell angles90.00, 103.67, 90.00
Refinement procedure
Resolution34.010 - 1.250
R-factor0.1936
Rwork0.193
R-free0.21230
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3b0b
RMSD bond length0.009
RMSD bond angle0.975
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwarePHENIX (1.18.2_3874)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]34.0101.295
High resolution limit [Å]1.2501.250
Rmerge0.0060.851
Rmeas0.0660.999
Rpim0.0340.520
Number of reflections436384340
<I/σ(I)>36.642.17
Completeness [%]96.796.21
Redundancy3.73.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.52930.1 M Tris-Bicine pH 8.5, 0.1 M Carboxylic acids mix, 12.5% MPD, 12.5% PEG 1000, 12.5% PEG 3350

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