7D98
Crystal structure of full-length CbnR complexed with the target DNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-1A |
Synchrotron site | Photon Factory |
Beamline | BL-1A |
Temperature [K] | 95 |
Detector technology | PIXEL |
Collection date | 2016-12-13 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 1.9000 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 105.819, 105.819, 602.516 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 3.600 |
R-factor | 0.237 |
Rwork | 0.234 |
R-free | 0.28610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1iz1 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.706 |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | PHENIX (1.18.2-3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 3.890 |
High resolution limit [Å] | 3.600 | 3.600 |
Rpim | 0.061 | 0.458 |
Number of reflections | 23984 | 4793 |
<I/σ(I)> | 12 | 2.1 |
Completeness [%] | 98.5 | |
Redundancy | 13.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 20%(w/v) PEG 3350, 0.5%(w/v) n-Octyl-pyranoside, 4%(v/v) Tacsimate |