7CZG
Crystal structure of FIP200 Claw domain apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-12-15 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97918 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 64.544, 75.616, 99.364 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.370 - 1.800 |
R-factor | 0.1912 |
Rwork | 0.189 |
R-free | 0.22950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6dce |
RMSD bond length | 0.006 |
RMSD bond angle | 0.797 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.170 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 41526 | 5232 |
<I/σ(I)> | 16.7 | |
Completeness [%] | 90.6 | |
Redundancy | 12.9 | |
CC(1/2) | 0.999 | 0.890 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | Sodium citrate tribasic dihydrate pH 5.0, Jeffamine ED-2001 pH 7.0 |