7CY1
Crystal Structure of MglC from Myxococcus xanthus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 11.2C |
Synchrotron site | ELETTRA |
Beamline | 11.2C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-02-26 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.98000 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 96.910, 96.910, 58.050 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 27.980 - 2.190 |
R-factor | 0.1904 |
Rwork | 0.188 |
R-free | 0.22690 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7ct3 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.462 |
Data reduction software | iMOSFLM (7.2.2) |
Data scaling software | Aimless (0.7.3) |
Phasing software | PHASER (2.8.2) |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 27.980 | 27.980 | 2.260 |
High resolution limit [Å] | 2.190 | 9.040 | 2.190 |
Rmerge | 0.075 | 0.025 | 0.959 |
Total number of observations | 154682 | 2076 | 11159 |
Number of reflections | 8534 | 151 | 708 |
<I/σ(I)> | 26.1 | 69.5 | 3.9 |
Completeness [%] | 98.8 | 95.2 | 97.2 |
Redundancy | 18.1 | 13.7 | 15.8 |
CC(1/2) | 1.000 | 1.000 | 0.885 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 291.15 | 2.8 M Sodium Acetate Trihydrate pH 7.0 |