7CUD
Crystal structure of HID in the unbound form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
Synchrotron site | Photon Factory |
Beamline | AR-NE3A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-02-18 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 63 |
Unit cell lengths | 76.070, 76.070, 33.920 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.180 - 1.800 |
R-factor | 0.1569 |
Rwork | 0.155 |
R-free | 0.20570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6dkq |
RMSD bond length | 0.013 |
RMSD bond angle | 1.715 |
Data reduction software | MOSFLM (7.1.0) |
Data scaling software | SCALA (3.3.21) |
Phasing software | PHASER (2.8.2) |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.900 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.133 | 0.524 |
Number of reflections | 10571 | 1545 |
<I/σ(I)> | 14.5 | 4.6 |
Completeness [%] | 99.8 | |
Redundancy | 10.8 | |
CC(1/2) | 0.997 | 0.907 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293.15 | 20% PEG-MME 2000 (20% w/v), 150mM KBr, 20mM TRIS-HCl |