7CQL
Apo GmaS without ligand
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-01-05 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 115.909, 179.024, 192.231 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.573 - 2.801 |
R-factor | 0.203 |
Rwork | 0.200 |
R-free | 0.25130 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4lni |
RMSD bond length | 0.009 |
RMSD bond angle | 1.216 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.6.4_486) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.900 |
High resolution limit [Å] | 2.800 | 6.034 | 2.800 |
Rmerge | 0.128 | 0.073 | 0.310 |
Rmeas | 0.134 | 0.077 | 0.325 |
Rpim | 0.040 | 0.022 | 0.099 |
Total number of observations | 545098 | ||
Number of reflections | 48331 | 5064 | 4782 |
<I/σ(I)> | 15.4 | ||
Completeness [%] | 98.6 | 98.8 | 99.1 |
Redundancy | 11.3 | 12.1 | 10.7 |
CC(1/2) | 0.998 | 0.985 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | 0.1 M MES (pH 6.5), 1 M lithium sulfate |