7CQ2
Crystal structure of Slx1-Slx4
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-07-19 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9792 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 61.284, 75.960, 186.966 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 42.486 - 2.500 |
| R-factor | 0.2044 |
| Rwork | 0.201 |
| R-free | 0.26230 |
| Structure solution method | SAD |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.740 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.7.3_928) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 50.000 | 50.000 | 2.590 |
| High resolution limit [Å] | 2.500 | 5.380 | 2.500 |
| Rmerge | 0.104 | 0.070 | 0.383 |
| Number of reflections | 58698 | 3373 | 3076 |
| <I/σ(I)> | 9.4 | ||
| Completeness [%] | 99.3 | 98.9 | 98.3 |
| Redundancy | 5.5 | 5.4 | 5.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.2 M potassium sodium tartrate tetrahydrate, 0.1M sodium cacodylate trihydrate, 20% PEG 3350 and 0.2 M NDSB-201 |
