7CPM
CRYSTAL STRUCTURE OF DODECAPRENYL DIPHOSPHATE SYNTHASE FROM THERMOBIFIDA FUSCA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-11-07 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.862, 137.590, 168.854 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.409 - 2.600 |
Rwork | 0.189 |
R-free | 0.23360 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1f75 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.369 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.409 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.056 | 0.371 |
Number of reflections | 52305 | 5149 |
<I/σ(I)> | 46.201 | 5.124 |
Completeness [%] | 99.8 | 100 |
Redundancy | 7.3 | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 298 | 0.1 M citric acid sodium citrate, 5% PEG6000 |