7CLF
PigF with SAH
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U1 |
| Synchrotron site | SSRF |
| Beamline | BL17U1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-04-16 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.0087 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 43.900, 109.200, 63.900 |
| Unit cell angles | 90.00, 93.10, 90.00 |
Refinement procedure
| Resolution | 19.675 - 1.982 |
| Rwork | 0.188 |
| R-free | 0.24890 |
| Structure solution method | SAD |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.730 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | CRANK2 |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.100 |
| High resolution limit [Å] | 1.980 | 1.980 |
| Rmeas | 0.144 | 0.936 |
| Number of reflections | 41497 | 6708 |
| <I/σ(I)> | 10.53 | 2 |
| Completeness [%] | 99.5 | 99.6 |
| Redundancy | 3.77 | |
| CC(1/2) | 0.995 | 0.707 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 295 | MPD |
