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7CLE

Non-Specific Class-c acidphosphatase from Sphingobium sp. RSMS

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsRRCAT INDUS-2 BEAMLINE PX-BL21
Synchrotron siteRRCAT INDUS-2
BeamlinePX-BL21
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2018-10-05
DetectorMAR scanner 300 mm plate
Wavelength(s)0.979500
Spacegroup nameI 41 3 2
Unit cell lengths170.622, 170.622, 170.622
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution42.656 - 2.342
R-factor0.1931
Rwork0.192
R-free0.22310
Structure solution methodAB INITIO PHASING
RMSD bond length0.003
RMSD bond angle0.617
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwareMR-Rosetta
Refinement softwarePHENIX (1.11.1_2575)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]45.6002.420
High resolution limit [Å]2.3402.340
Number of reflections180611632
<I/σ(I)>15.7
Completeness [%]99.4
Redundancy28.9
CC(1/2)0.9980.998
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1MICROBATCH5.52941M Ammonium sulphate, 0.1 M Bis-tris pH 5.5, 1% PEG 3350

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