7CJY
Drimenol synthase from Persicaria hydropiper
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-17 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.979 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 232.530, 60.090, 106.220 |
Unit cell angles | 90.00, 111.88, 90.00 |
Refinement procedure
Resolution | 28.740 - 2.200 |
R-factor | 0.1966 |
Rwork | 0.195 |
R-free | 0.23380 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5eau |
RMSD bond length | 0.008 |
RMSD bond angle | 0.953 |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.740 | 2.279 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.086 | 0.568 |
Rmeas | 0.094 | 0.616 |
Rpim | 0.037 | 0.237 |
Number of reflections | 69159 | 6797 |
<I/σ(I)> | 12.09 | 2.72 |
Completeness [%] | 99.0 | 98.56 |
Redundancy | 6.6 | 6.8 |
CC(1/2) | 0.995 | 0.961 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 22.5% w/v PEG 3000, 0.1 M citrate, pH 5.5, 0.2 M ammonium acetate, 10% v/v glycerol |