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7CJ7

Crystal structure of homo dimeric D-allulose 3-epimerase from Methylomonas sp. in complex with L-tagatose

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-17A
Synchrotron sitePhoton Factory
BeamlineBL-17A
Temperature [K]100
Detector technologyPIXEL
Collection date2019-03-25
DetectorDECTRIS EIGER X 16M
Wavelength(s)0.98
Spacegroup nameP 21 21 21
Unit cell lengths46.056, 81.777, 140.033
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution39.250 - 1.695
R-factor0.1501
Rwork0.148
R-free0.19000
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)5zfs
RMSD bond length0.005
RMSD bond angle1.209
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0258)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0001.730
High resolution limit [Å]1.6904.6101.700
Rmerge0.1140.0450.635
Rmeas0.1260.0510.691
Rpim0.0520.0220.269
Number of reflections5867131762875
<I/σ(I)>7
Completeness [%]98.698.398.4
Redundancy5.65.16.1
CC(1/2)0.9970.851
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.5293PEG3350, Tris, magnesium chloride

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