7CJ0
Crystal structure of DNAJC9 HBD in complex with H3.3-H4 dimer and MCM2 HBD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-11-23 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 47.510, 47.510, 616.260 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.080 - 2.500 |
R-factor | 0.2607 |
Rwork | 0.258 |
R-free | 0.29480 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5bnv |
RMSD bond length | 0.002 |
RMSD bond angle | 0.445 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 41.084 | 41.080 | 2.300 |
High resolution limit [Å] | 2.240 | 10.020 | 2.240 |
Rmerge | 0.086 | 0.043 | 2.034 |
Number of reflections | 41413 | 621 | 2958 |
<I/σ(I)> | 17.7 | ||
Completeness [%] | 99.9 | 99 | 99.1 |
Redundancy | 17.3 | 13.7 | 16.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.17 M Sodium acetate, 0.1 M Tris, pH8.5, 25% (v/v) PEG 4000, 20% (v/v) Glycerol |