7C3O

Crystal structure of TT109 from CANDIDA ALBICANS

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	CCD
Collection date	2014-07-01
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	1.000
Spacegroup name	P 1 21 1
Unit cell lengths	51.754, 70.036, 54.559
Unit cell angles	90.00, 114.32, 90.00

Refinement procedure

Resolution	25.820 - 1.890
R-factor	0.1667
Rwork	0.165
R-free	0.19190
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	7bxw
RMSD bond length	0.010
RMSD bond angle	1.218
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Refinement software	PHENIX (1.17.1_3660)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.970
High resolution limit [Å]	1.890	1.890
Number of reflections	107314	107314
<I/σ(I)>	6.85
Completeness [%]	98.9
Redundancy	3.8
CC(1/2)	0.990	0.960

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		289	PEG