Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

7C10

Dithiol cGrx1

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPAL/PLS BEAMLINE 5C (4A)
Synchrotron sitePAL/PLS
Beamline5C (4A)
Temperature [K]100
Detector technologyPIXEL
Collection date2018-07-03
DetectorDECTRIS EIGER2 X 9M
Wavelength(s)1
Spacegroup nameC 1 2 1
Unit cell lengths93.420, 61.105, 93.940
Unit cell angles90.00, 104.24, 90.00
Refinement procedure
Resolution37.069 - 2.806
R-factor0.2248
Rwork0.219
R-free0.27540
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4tr1
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHENIX
Refinement softwarePHENIX (1.16_3549)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0002.850
High resolution limit [Å]2.8007.5902.800
Rmerge0.0470.0300.126
Rmeas0.0510.0330.142
Rpim0.0200.0130.064
Total number of observations71066
Number of reflections12448605580
<I/σ(I)>33.7
Completeness [%]98.190.295.1
Redundancy5.76.34.2
CC(1/2)0.9990.985
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP2930.1M sodium phosphate/citric acid pH4.2, 0.2M Lithium sulfate, 20% PEG 1000

226707

PDB entries from 2024-10-30

PDB statisticsPDBj update infoContact PDBjnumon