7C0Q
a Legionella pneumophila effector Lpg2505
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 233 |
Detector technology | PIXEL |
Collection date | 2018-12-30 |
Detector | DECTRIS PILATUS3 R CdTe 300K |
Wavelength(s) | 0.9792 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 106.542, 50.448, 122.029 |
Unit cell angles | 90.00, 109.06, 90.00 |
Refinement procedure
Resolution | 92.236 - 2.600 |
R-factor | 0.2309 |
Rwork | 0.229 |
R-free | 0.27550 |
Structure solution method | SAD |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 92.236 | 2.640 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 35768 | 37795 |
<I/σ(I)> | 14.227 | |
Completeness [%] | 98.2 | 99.2 |
Redundancy | 6.9 | 7.2 |
CC(1/2) | 0.995 | 0.721 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.1 M HEPES pH 7.5, 25% PEG 3350 |