7C0G
Aca1 in complex with 14bp palindromic DNA target
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-10-15 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97890 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 68.727, 68.727, 206.006 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.000 - 2.400 |
R-factor | 0.2201 |
Rwork | 0.217 |
R-free | 0.26890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7C0B |
RMSD bond length | 0.011 |
RMSD bond angle | 1.413 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (phenix-1.16-3549) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.133 | 0.814 |
Number of reflections | 12045 | 1108 |
<I/σ(I)> | 24.333 | |
Completeness [%] | 99.5 | |
Redundancy | 27.4 | |
CC(1/2) | 1.000 | 0.385 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M Sodium acetate pH5.0; 20%(w/v) MPD |