7BY1
Crystal structure of GCN5 PCAF N-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-1A |
Synchrotron site | Photon Factory |
Beamline | BL-1A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-18 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.1000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 43.069, 148.857, 58.998 |
Unit cell angles | 90.00, 101.03, 90.00 |
Refinement procedure
Resolution | 45.700 - 1.800 |
R-factor | 0.1978 |
Rwork | 0.196 |
R-free | 0.23148 |
Structure solution method | SAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.777 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHARP |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.700 | 1.840 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 67271 | 28263 |
<I/σ(I)> | 14.7 | |
Completeness [%] | 100.0 | |
Redundancy | 7 | |
CC(1/2) | 0.998 | 0.794 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 100 mM imidazole/MES (pH 6.5), 20% PEGMME500, 10% PEG20,000 , 20 mM sodium formate , 20 mM ammonium acetate, 20 mM sodium citrate tribasic dehydrate, 20 mM sodium potassium tartrate tetrahydrate, 20 mM sodium oxamate |