7BVO

Crystal structure of lysozyme delivered in alginate

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 11C
Synchrotron site	PAL/PLS
Beamline	11C
Temperature [K]	298.15
Detector technology	PIXEL
Collection date	2019-06-11
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9795
Spacegroup name	P 43 21 2
Unit cell lengths	79.450, 79.450, 38.470
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	56.180 - 1.900
R-factor	0.1926
Rwork	0.190
R-free	0.23820
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6ig6
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX (1.15.2_3472)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	80.000	1.970
High resolution limit [Å]	1.900	1.900
Number of reflections	10209	989
<I/σ(I)>	3.91	1.31
Completeness [%]	100.0	100
Redundancy	158.1	112.7
CC(1/2)	0.967	0.442

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	SMALL TUBES		293.5	sodium acetate, PEG 8000, NaCl