7BVL
Crystal structure of glucose isomerase delivered in wheat starch
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 11C |
Synchrotron site | PAL/PLS |
Beamline | 11C |
Temperature [K] | 298.15 |
Detector technology | PIXEL |
Collection date | 2019-05-09 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 94.490, 99.920, 100.190 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 70.749 - 2.000 |
R-factor | 0.1731 |
Rwork | 0.171 |
R-free | 0.21300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5zyd |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.400 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 33248 | 3247 |
<I/σ(I)> | 4.01 | |
Completeness [%] | 100.0 | |
Redundancy | 148.5 | |
CC(1/2) | 0.976 | 0.597 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 7 | 293.5 | Tris-HCl, Ammonium sulfate, Magnesium sulfate |