7BV0

HEV-C E2s

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	FREE ELECTRON LASER
Source details	PAL-XFEL BEAMLINE NCI
Synchrotron site	PAL-XFEL
Beamline	NCI
Temperature [K]	293
Detector technology	CCD
Collection date	2019-10-09
Detector	Nonius Kappa CCD
Wavelength(s)	0.988
Spacegroup name	P 63 2 2
Unit cell lengths	107.660, 107.660, 75.458
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	46.618 - 1.801
R-factor	0.1718
Rwork	0.171
R-free	0.18810
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3ggq
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX (1.15.2_3472)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	46.618	1.874
High resolution limit [Å]	1.801	1.801
Number of reflections	24297	24297
<I/σ(I)>	1
Completeness [%]	99.7	99
Redundancy	20
CC(1/2)	0.750	0.500

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	BATCH MODE		293.5	0.1 M sodium acetate trihydrate pH 4.5, 3.0 M sodium chloride