7BU9
Crystal Structure of Spindlin1-H3(K4me3-K9me2) complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-02-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97918 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.471, 143.783, 129.990 |
Unit cell angles | 90.00, 95.86, 90.00 |
Refinement procedure
Resolution | 48.074 - 3.502 |
R-factor | 0.2466 |
Rwork | 0.246 |
R-free | 0.26420 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ns2 |
Data reduction software | DENZO |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3247) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.560 |
High resolution limit [Å] | 3.500 | 9.480 | 3.500 |
Rmerge | 0.153 | 0.068 | 0.490 |
Rmeas | 0.181 | 0.081 | 0.578 |
Rpim | 0.096 | 0.043 | 0.304 |
Total number of observations | 64751 | ||
Number of reflections | 18492 | 968 | 930 |
<I/σ(I)> | 4.5 | ||
Completeness [%] | 98.9 | 99.4 | 99.9 |
Redundancy | 3.5 | 3.4 | 3.6 |
CC(1/2) | 0.996 | 0.812 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 291 | 3.6M sodium formate, 3% DMSO |