7BQA
Crystal structure of ASFV p35
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-11 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.071460 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 58.068, 89.563, 65.080 |
Unit cell angles | 90.00, 89.95, 90.00 |
Refinement procedure
Resolution | 48.723 - 2.102 |
R-factor | 0.2033 |
Rwork | 0.200 |
R-free | 0.22760 |
Structure solution method | SAD |
Data reduction software | HKL-3000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.140 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 37964 | 1940 |
<I/σ(I)> | 10.7 | |
Completeness [%] | 97.8 | |
Redundancy | 5.8 | |
CC(1/2) | 0.966 | 0.862 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.1M BIS-TRIS pH 6.0, 30% W/V Polyethylene glycol 3350 |