7BOO
Crystal Structure of Core-mannan synthase A (CmsA/Ktr4) from Aspergillus fumigatus, apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-20 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 154.719, 274.296, 185.974 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.990 - 1.950 |
R-factor | 0.1644 |
Rwork | 0.163 |
R-free | 0.18594 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5a07 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.290 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.990 | 2.020 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.062 | 0.555 |
Rmeas | 0.067 | 0.600 |
Number of reflections | 284394 | 27979 |
<I/σ(I)> | 19.22 | 3.38 |
Completeness [%] | 99.8 | |
Redundancy | 7 | |
CC(1/2) | 0.999 | 0.897 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | sodium citrate |