7BGO
The crystal structure of gene product PA4063 from Pseudomonas aeruginosa in complex with Zn (space group P65)
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 11.2C |
Synchrotron site | ELETTRA |
Beamline | 11.2C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-12-12 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.27110 |
Spacegroup name | P 65 |
Unit cell lengths | 122.005, 122.005, 102.263 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.940 - 3.301 |
Rwork | 0.177 |
R-free | 0.21140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7aly |
RMSD bond length | 0.010 |
RMSD bond angle | 1.785 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | AutoSol |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.940 | 46.940 | 3.570 |
High resolution limit [Å] | 3.300 | 8.730 | 3.300 |
Rmerge | 0.135 | 0.030 | 2.461 |
Rmeas | 0.143 | 0.032 | 2.608 |
Rpim | 0.047 | 0.011 | 0.860 |
Number of reflections | 12599 | 733 | 2650 |
<I/σ(I)> | 18.6 | ||
Completeness [%] | 96.1 | ||
Redundancy | 17.7 | 15.8 | 17.9 |
CC(1/2) | 0.999 | 1.000 | 0.677 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294 | AS 3M, MPD 1% |