7BEW
Glyceraldehyde 3-phosphate dehydrogenase from Campylobacter jejeuni - NAD(P) complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-12-02 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 90.810, 90.810, 224.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 57.797 - 2.250 |
Rwork | 0.163 |
R-free | 0.21180 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.010 |
RMSD bond angle | 1.674 |
Data reduction software | xia2 |
Data scaling software | SCALA |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 64.210 | 2.350 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmerge | 0.150 | 0.730 |
Number of reflections | 22791 | 1658 |
<I/σ(I)> | 10.6 | 2.5 |
Completeness [%] | 99.9 | 100 |
Redundancy | 6.5 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 295 | PEG 4000 (20%), 0.3 M Na/K tartrate, 01.M Na Acetate |