7BEC
Unusual structural features in the adduct of dirhodium tetraacetate with lysozyme (5)
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-24 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.700, 78.700, 37.245 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.190 - 1.740 |
Rwork | 0.185 |
R-free | 0.22840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 193l |
RMSD bond length | 0.008 |
RMSD bond angle | 1.553 |
Data reduction software | MOSFLM |
Data scaling software | MOSFLM |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.190 | 1.830 |
High resolution limit [Å] | 1.740 | 1.740 |
Rmerge | 0.070 | 3.120 |
Rpim | 0.020 | 0.848 |
Number of reflections | 11349 | 567 |
<I/σ(I)> | 24.7 | 1.1 |
Completeness [%] | 91.1 | 36 |
Redundancy | 25 | 27.6 |
CC(1/2) | 1.000 | 0.474 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 293 | 0.1 M sodium acetate, 20% ethylene glicol, 0.1 M sodium nitrate |