7BEB
Unusual structural features in the adduct of dirhodium tetraacetate with lysozyme (4)
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-24 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.604, 78.604, 37.307 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.580 - 1.320 |
Rwork | 0.178 |
R-free | 0.22330 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 193l |
RMSD bond length | 0.013 |
RMSD bond angle | 2.394 |
Data reduction software | MOSFLM |
Data scaling software | MOSFLM |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.580 | 1.370 |
High resolution limit [Å] | 1.320 | 1.320 |
Rmerge | 0.047 | 2.550 |
Rpim | 0.013 | 0.720 |
Number of reflections | 26513 | 1327 |
<I/σ(I)> | 28.8 | |
Completeness [%] | 95.4 | 51.1 |
Redundancy | 25.8 | 25.9 |
CC(1/2) | 1.000 | 0.612 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 293 | 0.1 M sodium acetate, 20% ethylene glicol, 0.6 M sodium nitrate |