7BEB

Unusual structural features in the adduct of dirhodium tetraacetate with lysozyme (4)

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-01-24
Detector	DECTRIS PILATUS 6M-F
Wavelength(s)	0.9795
Spacegroup name	P 43 21 2
Unit cell lengths	78.604, 78.604, 37.307
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	55.580 - 1.320
Rwork	0.178
R-free	0.22330
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	193l
RMSD bond length	0.013
RMSD bond angle	2.394
Data reduction software	MOSFLM
Data scaling software	MOSFLM
Phasing software	PHASER
Refinement software	REFMAC (5.8.0258)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	55.580	1.370
High resolution limit [Å]	1.320	1.320
Rmerge	0.047	2.550
Rpim	0.013	0.720
Number of reflections	26513	1327
<I/σ(I)>	28.8
Completeness [%]	95.4	51.1
Redundancy	25.8	25.9
CC(1/2)	1.000	0.612

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.5	293	0.1 M sodium acetate, 20% ethylene glicol, 0.6 M sodium nitrate