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7BC8

Notum Fragment 658

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04-1
Synchrotron siteDiamond
BeamlineI04-1
Temperature [K]100
Detector technologyPIXEL
Collection date2017-02-02
DetectorDECTRIS PILATUS3 S 6M
Wavelength(s)0.9282
Spacegroup nameP 21 21 21
Unit cell lengths59.728, 73.312, 78.537
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution53.590 - 1.740
R-factor0.2168
Rwork0.216
R-free0.23850
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4uzq
Data reduction softwarexia2
Data scaling softwarexia2
Phasing softwareMOLREP
Refinement softwarePHENIX (1.18.2_3874)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]59.7301.770
High resolution limit [Å]1.7401.740
Number of reflections361011743
<I/σ(I)>8.5
Completeness [%]100.0
Redundancy6.3
CC(1/2)1.0000.510
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2961.5 M Ammonium Sulphate 0.1 M Sodium Citrate, pH4.2

229183

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